Coordination Compounds

Complete JEE & NEET Preparation Notes

Werner's Theory

JEE Focus: Primary vs Secondary Valence, Coordination Number, Isomerism

Key Postulates:

  • Metals show two types of linkages: Primary valence (ionizable, oxidation state) and Secondary valence (non-ionizable, coordination number)
  • Secondary valence is fixed for a metal and determines geometry
  • Characteristic spatial arrangements → Coordination polyhedra

Experimental Evidence:

Compound AgCl precipitated Coordination Entity
CoCl₃·6NH₃ (Yellow) 3 mol [Co(NH₃)₆]³⁺ 3Cl⁻
CoCl₃·5NH₃ (Purple) 2 mol [CoCl(NH₃)₅]²⁺ 2Cl⁻
CoCl₃·4NH₃ (Green/Violet) 1 mol [CoCl₂(NH₃)₄]⁺ Cl⁻

Important Definitions

Coordination Entity:

Central metal + attached ligands
Example: [Co(NH₃)₆]³⁺, [Fe(CN)₆]⁴⁻

Ligands Classification:

Type Denticity Examples
Unidentate 1 NH₃, H₂O, Cl⁻, CO
Didentate 2 en (ethane-1,2-diamine), ox²⁻ (oxalate)
Polydentate >2 EDTA⁴⁻ (hexadentate), dien
Ambidentate 1 (two donor atoms) NO₂⁻ (N or O), SCN⁻ (S or N)

Coordination Number (CN):

Number of ligand donor atoms directly bonded to metal

[PtCl₆]²⁻ → CN = 6
[Ni(NH₃)₄]²⁺ → CN = 4
[Fe(C₂O₄)₃]³⁻ → CN = 6 (oxalate is didentate)

Nomenclature Rules

Writing Formulas:

  • Central atom first
  • Ligands in alphabetical order (ignore prefixes)
  • Entire complex in square brackets
  • Charge indicated as superscript

Naming Complexes:

  • Cation named before anion
  • Ligands in alphabetical order before metal
  • Anionic ligands end in '-o'
  • Oxidation state in Roman numerals
  • If complex is anion, metal name ends in '-ate'
Examples:
[Cr(NH₃)₃(H₂O)₃]Cl₃ → triamminetriaquachromium(III) chloride
K₃[Cr(C₂O₄)₃] → potassium trioxalatochromate(III)
[CoCl₂(en)₂]⁺ → dichloridobis(ethane-1,2-diamine)cobalt(III)

Isomerism in Coordination Compounds

Structural Isomerism:

  • Linkage: Ambidentate ligands (NO₂⁻ → nitro vs nitrito)
  • Coordination: Ligand exchange between cation & anion
  • Ionisation: Counter ion exchange ([Co(NH₃)₅SO₄]Br vs [Co(NH₃)₅Br]SO₄)
  • Solvate/Hydrate: Water inside/outside coordination sphere

Stereoisomerism:

Geometrical Isomerism:

Square planar [MX₂L₂]: cis & trans isomers
Octahedral [MX₂L₄]: cis & trans isomers
Octahedral [MA₃B₃]: fac & mer isomers

Optical Isomerism:

  • Mirror images that are non-superimposable
  • Common with chelating ligands
  • Example: [Co(en)₃]³⁺ shows d and l forms
NEET Tip: Optical activity requires molecular chirality - no plane of symmetry

Bonding Theories

Valence Bond Theory (VBT):

Coordination Number Hybridization Geometry Examples
4 sp³ Tetrahedral [NiCl₄]²⁻
4 dsp² Square planar [Ni(CN)₄]²⁻
6 sp³d² Octahedral (outer orbital) [CoF₆]³⁻
6 d²sp³ Octahedral (inner orbital) [Co(NH₃)₆]³⁺

Crystal Field Theory (CFT):

Octahedral Splitting: t₂g (lower) and e_g (higher) orbitals
Splitting Energy: Δ₀

Spectrochemical Series:
I⁻ < Br⁻ < SCN⁻ < Cl⁻ < S²⁻ < F⁻ < OH⁻ < C₂O₄²⁻ < H₂O < NCS⁻ < edta⁴⁻ < NH₃ < en < CN⁻ < CO
JEE Focus: Strong field ligands cause large Δ₀ → low spin complexes
Weak field ligands cause small Δ₀ → high spin complexes

Properties & Applications

Magnetic Properties:

  • Paramagnetic: Unpaired electrons
  • Diamagnetic: All electrons paired
  • Magnetic moment = √[n(n+2)] BM (n = unpaired electrons)

Color in Coordination Compounds:

Due to d-d transitions when Δ matches visible light energy

[Ti(H₂O)₆]³⁺: d¹, absorbs green → appears violet
Color depends on: Metal ion, Oxidation state, Ligands

Important Applications:

  • Biological: Chlorophyll (Mg), Hemoglobin (Fe), Vitamin B₁₂ (Co)
  • Analytical: EDTA titrations, Qualitative analysis
  • Industrial: Catalysts, Electroplating, Photography
  • Medical: Cisplatin (anti-cancer), Chelation therapy
  • Metallurgical: Extraction of Au, Ag using CN⁻ complexes

JEE/NEET Practice Questions

Question 1:

Which of the following complexes shows geometrical isomerism?

(a) [Co(NH₃)₆]³⁺ (b) [Pt(NH₃)₂Cl₂] (c) [Ni(CO)₄] (d) [Co(en)₃]³⁺

Answer: (b) [Pt(NH₃)₂Cl₂] - Square planar complex

Question 2:

The complex [Fe(CN)₆]³⁻ has one unpaired electron, while [FeF₆]³⁻ has five unpaired electrons. Explain using CFT.

Answer: CN⁻ is strong field ligand (large Δ₀) → low spin complex. F⁻ is weak field ligand (small Δ₀) → high spin complex.

Question 3:

Write IUPAC name: K₃[Fe(C₂O₄)₃]

Answer: Potassium trioxalatoferrate(III)

Exam Strategy:
• Memorize spectrochemical series
• Practice naming and formula writing
• Understand magnetic behavior predictions
• Know common biological coordination compounds